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Edited by:

Daniel Bonamy, Commissariat à l’Énergie Atomique et aux Énergies Alternatives, France Reviewed by:

Eric Josef Ribeiro Parteli, University of Erlangen-Nuremberg, Germany Ferenc Kun, University of Debrecen, Hungary

*Correspondence:

Benjy Marks, Condensed Matter Physics, Department of Physics, University of Oslo, Sem Sælands Vei 24, Fysikkbygningen, Oslo 0371, Norway benjy.marks@fys.uio.no

Specialty section:

This article was submitted to Interdisciplinary Physics, a section of the journal Frontiers in Physics Received:20 April 2015 Accepted:27 May 2015 Published:09 June 2015 Citation:

Marks B, Sandnes B, Dumazer G, Eriksen JA and Måløy KJ (2015) Compaction of granular material inside confined geometries.

Front. Phys. 3:41.

doi: 10.3389/fphy.2015.00041

Compaction of granular material inside confined geometries

Benjy Marks1, 2*, Bjørnar Sandnes2, Guillaume Dumazer1, Jon A. Eriksen1, 3and Knut J. Måløy1

1Condensed Matter Physics, Department of Physics, University of Oslo, Oslo, Norway,2College of Engineering, Swansea University, Swansea, UK,3Centre National de la Recherche Scientifique, Institut de Physique du Globe de Strasbourg, University of Strasbourg/Ecole et Observatoire des Sciences de la Terre, Strasbourg, France

In both nature and engineering, loosely packed granular materials are often compacted inside confined geometries. Here, we explore such behavior in a quasi-two dimensional geometry, where parallel rigid walls provide the confinement. We use the discrete element method to investigate the stress distribution developed within the granular packing as a result of compaction due to the displacement of a rigid piston. We observe that the stress within the packing increases exponentially with the length of accumulated grains, and show an extension to current analytic models which fits the measured stress. The micromechanical behavior is studied for a range of system parameters, and the limitations of existing analytic models are described. In particular, we show the smallest sized systems which can be treated using existing models. Additionally, the effects of increasing piston rate, and variations of the initial packing fraction, are described.

Keywords: granular material, Janssen stress, boundary effects, confinement, deformable media, hele-shaw cell, discrete element method, micromechanics

1. Introduction

When granular materials are placed in confined geometries, we often observe a significant portion of the stress being redirected toward the confining boundaries. This phenomenon has been systematically studied for many systems [1–3], most notably in silos, beginning with Janssen [4].

Force redirection has been attributed to the granular nature of the material, and has in many cases been shown to be well represented by a constant coefficient, known as the Janssen coefficientK, defined in one spatial dimension as

K=σrn,

whereσr is the redirected stress due to some applied normal stressσn. Here we investigate the development of stresses within a granular packing, confined vertically between two horizontal plates, with no walls in the remaining directions, subjected to a rigid piston impacting it from one side. As the piston moves, granular material is compacted near the piston, and with increasing displacement of the piston, the size of the packing increases. Such an accumulation process is known to occur in the petroleum industry, where sand is liberated from the host rock during extraction, altering the underground morphology of cracks [5, 6].

This may also be relevant for understanding proppant flowback in propped fractures [7].

Additionally, this geometry is representative of a number of recent experimental studies in Hele-Shaw cells [8–11] where the validity of Janssen stress redirection has not been ascertained.

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There are a number of interesting patterns which form when a granular material is displaced by a flexible interface in such a geometry [9,11]. The nature of the patterns have been shown to depend on many factors, primarily the initial packing fraction and the rate of displacement [10]. For this reason, we here investigate the microstructural and mechanical evolution of such a system under these conditions. To reduce the complexity of the system, we consider only a rigid piston.

We are interested in systems which are highly confined. In common experiments with granular material inside Hele-Shaw cells, there are in general fewer than 20 grain diameters between the two Hele-Shaw plates, typically down to around 5 grain diameters [10]. As the confinement increases, i.e., as the gap spacing decreases, we expect a transition from three dimensional behavior toward a behavior governed by the boundaries, as demonstrated for vertical silos in Bratberg et al. [12]. It is then of interest to study the changes that result from increasing confinement. We expect that altering the confinement will affect the force redistribution. A transition may occur for extremely confined systems where such an assumption concerning force redirection may not be valid.

Existing analytic models for the micromechanics of such a system generally reduce the problem to one spatial dimension (x), assuming that variations in both remaining directions (y and z) are small, although recently curved interfaces have also been described [8]. For simplicity, we consider a flat interface, and validate the analytic description with a discrete element model.

Firstly, in Section 2 describe the numerical model that has been used to simulate this system. In Section 3, we establish continuum properties which correspond to the analytic formulation, and show comparisons between the two. In particular, the limitations of current analytic models are identified. Finally, a parameter set is proposed that best fits the analytic theories for a wide range of system variables.

FIGURE 1 | Particle positions during a single test, shown at six piston displacements s. Top to bottom: s=0,10,20,30,40, and 50. Labels refer to the coordinate system x, y, and z, the gap

height D, the plug length L and the initial packing fraction φ0. Particles are colored by size, darker colors representing smaller particles.

2. Materials and Methods

This paper is an investigation into the micromechanics of a system which is highly constrained by external boundaries. For this reason, it is ideal to use a particle based method to model the behavior, as the total number of grains in the system is small. Toward this end, we use a conventional soft sphere discrete particle approach, implemented in the open source code MercuryDPM (www.mercurydpm.org) [13, 14]. The geometry considered here, shown inFigure 1, consists of a rigid piston, oriented in a spacer = {x,y,z}, with normal along thexaxis, which pushes particles between two rigid plates, separated by a spacingD and having normals in the±z directions, with two periodic boundaries in the remaining perpendicular direction, y. The coordinate system moves with the piston, such that it is located atx=0 at all times. As the piston moves horizontally at a velocityutoward the grains, its displacement at any timetis then s=ut.

We work in a system of non-dimensionalized units with the following properties; length and mass have been non- dimensionalized by the lengthdm and mass mm of the largest particle in the system, respectively, where the prime indicates that the quantity has dimension. The particle diameters,d, we use are therefore d ≤ 1, with material density defined by 4π(1/2)3ρp/3= 1, orρp =6/π. Time is non-dimensionalized by the time taken for the largest particle to fall from rest its own radius under the action of gravity, so that a unit time is t = p

dm/g, which requires that g = 1. Other values are non-dimensionalized by a combination of these three scales, for example stress is non-dimensionalized bymmg/d′2m.

Particles are filled into the available space by assigning them to positions on a regular hexagonally close packed lattice, dimensioned such that particles of diameter 1 would be in contact. In all cases we use particles distributed uniformly in the range 0.5 ≤ d ≤ 1 to avoid crystallization, and to mimic the size range used in Sandnes et al. [10]. Variable particle filling is

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facilitated by changing the number of layers of the grid, such that the initial packing fraction,φ0 defined in Equation (3), is approximately constant throughout the cell. Fromt = −10 to t = 0, gravity in the−z direction is increased fromg = 0 to g = 1 to settle the grains in a loose packing. Fromt = 0 the piston begins to move at velocityu.

As shown in Figure 2, the particles’ material properties are described by normal, tangential and rolling damped spring sliders [13,15] with the properties contained inTable 1. These values have previously been calibrated to mimic 20 micron silica beads [16]. Here we neglect the role of adhesion between particles, which will become increasingly important as the physical size of the particles reduces. The walls are implemented such that they are rough; when a particle contacts a wall, the piston, or both, it is prohibited from rotating, i.e., µr = 1.

Otherwise, the interaction properties are the same as between two particles, except that the walls and piston are of infinite mass.

We therefore have a well defined macroscopic sliding friction of µ=0.4 that does not depend on the rate of loading.

In the following Section we will firstly detail the important macroscopic quantities measured from a single simulation. We will then investigate the effect of three controlling parameters on the evolution of the system: the Hele-Shaw spacingD, the initial packing fractionφ0and the velocity of the piston,u. The piston

FIGURE 2 | Contact laws used in the discrete element model.

Interactions are characterized by(A)normal,(B)tangential and(C)rolling laws, parameterized by stiffnessesk,ktandkr, viscous dissipationγ,γtandγr and friction coefficientsµtandµr. Full details are given in Luding [15].

TABLE 1 | Material properties of the spheres.

Direction Stiffness,k Dissipation,γ Coefficient of friction,µ kg/s2

m m/(gd

m)

kg/s m

m/ qgd

m

Normal 1,00000 1000

Tangential 80,000 0 0.4

Rolling 80,000 0 10−3

rate, however, is nota prioria governing quantity, so we choose to control the piston rate via the inertial number,I, which is defined asI = ˙γdm/p

P/ρp, which is the ratio of inertial to imposed stresses, wherePis a typical pressure andγ˙ is a typical shear strain rate [17]. Takingγ˙=u/D, andP=ρpgD, gives

I= udm

D3/2g1/2 =uD−3/2.

3. Results

As depicted inFigure 1, three distinct regions exist inside the system. These are termed the plug zone, where particles are densely packed near to the piston (x≤L), theundisturbed zone, far from the plug, and thetransition zone, where the plug is accumulating. To define these regions systematically, we must first measure the solid fraction, ν = Vs/Vt, which is a local measure of the ratio of the volume of solids to the total volume.

The solid fraction is coarse grained in one spatial dimension,x, as ν(x,t)= 1

WD

N

X

i=1

ViW(x−xi(t)), (1) where N is the number of grains in the system, W is the width of the system,Vi is the volume of thei-th grain,xi its center of mass andW is the coarse graining function, chosen in this case to be a 1D normalized Gaussian function [14,18].

Such a coarse graining method allows the coarse graining width to be defined, so that either the macro- or micro-structure is visible. We choose to use a coarse graining width equal to the maximum particle diameter, such that small scale variations are minimized, and smooth continuum fields are obtained [19]. All other continuum quantities are defined using the same coarse graining technique, presented in Goldhirsch [18], Weinhart et al.

[14]. Using the definition (1), we denote the maximum solid fraction,νm, as an average over the solid fraction close to the wall at some time when the transition zone is far from the piston as

νm= 1 5D

Z 10D

5D

ν(x)dx, (2)

where in practice a numerical integration is done over the discrete coarse grained cells, and the limits of 5Dand 10Dare chosen arbitrarily. We define the normalized packing fraction, φ(x,t), asφ =ν/νm, and note that in the absence of volumetric expansion or dilation of the granular material, φ is directly proportional to the height of the packing between the Hele-Shaw walls. The undisturbed zone is that which is maintained at the initial packing fractionφ0, which is defined at timet=0 as

φ0= 1 5D

Z 10D

5D

φ(x,t=0)dx.

To delineate the plug, transition and undisturbed zones, at each timet we use linear regression to find the best linear fit to the

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points in the range φ = φ0 + 0.1 to φ = 0.9, such that φD ≈ b−xtanθ, for some value ofband slope angleθ. Five examples of this are shown inFigure 3A. Using this best fit, we can define the point at which the plug zone meets the transition zone as the intersection of the best fit regression line andφ=1, such thatL=(b−D)/tanθ, as shown inFigure 3A. The value ofLgrows monotonically with piston displacement, as shown in Figure 3B. Conservation of mass implies that on average, if there is no volumetric change in the packing, and no slip between the grains and the walls, this relationship can be expressed as

L s = φ0

1−φ0, (3)

which is shown as the dashed line in Figure 3B. For all cases reported here, the value of θ does not appear to vary with increasing plug length L. The point at which the undisturbed zone meets the transition zone can then be defined in a similar manner as above, by the intersection of the

best fit regression line with φ = φ0. The coordination number, Z, (average number of contacts per particle), is fairly constant in the plug zone, (Figure 3C), increasing with compaction, as rearrangement occurs. Additionally, at large values of L the stresses are high enough to cause significant overlap of the particles (up to 1%). In the transition zone, significant particle rearrangement lowers the coordination number.

Coarse graining techniques in general cause measured fields to converge toward zero near boundaries [14]. While it is feasible to reconstruct these fields in general near individual boundaries, near the piston we have three distinct boundaries which all interact. To access stresses in this region, it is then preferable to directly measure the forces applied to the rigid boundaries of the system. Toward this end, we denoteσnp as the normal stress measured at the piston. This is shown as a function of piston displacement inFigure 3D. The stresses measured from coarse graining within the packing are shown inFigure 3E. In both cases, the stresses grow exponentially both with increasing

FIGURE 3 | Evolution of coarse grained properties of the system with increasing piston displacement,s, forD=5,φ0=0.5and I=0.01. (A)Five examples of the normalized packing fraction of the particles,φ. The magenta, red, green, blue, and black lines indicate displacements which correspond toL=0,12.5,25,37.5, and 50 respectively. The same color scheme is used for each subsequent plot in this Figure unless stated otherwise. A filled circle indicates the measured value ofL, and the cyan dashed line indicates the linear best fit measurement of the transition zone.(B)Evolution of the measured value ofLwith increasing displacementsdrawn in black. The cyan line

indicates the best linear fit to these points.(C)The coordination number, Z, as a function of normalized distance from the piston head,x/L.(D) Normal stress measured at the piston is shown in black. The cyan dashed line indicates the best fit estimate of Equation (6).(E)Normal stress distributions within the packing. Solid lines indicateσxx, dashedσyy and dottedσzz.(F)Apparent friction coefficient measured within the packing,µ= |σxz|/σzz.(G)Out of plane Janssen coefficient measured within the packing,Ky=σyyxx.(H)In plane vertical Janssen coefficient measured within the packing,Kz=zzρpνgD/2)/σxx.(I)Absolute value of thexcomponent of the eigenvector of the major principal stress.

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Land decreasingx, as shown by the linearity in a semilog space inFigures 3D,E.

An analytic expression to describe this stress evolution was first derived in Knudsen et al. [9], assuming that: (a) the stress redirection in thez direction is described by a constantKz = σzzxx, where σzz = σzz −Dρpνmg/2 is the component of the vertical stress not due to gravity and (b) friction at the side walls isµ = σxyzz. It can be shown using force balance in the xdirection that under these conditions, if there is no net acceleration,

xx

dx = −2µKz

D σxx−µρpνmg.

By further assuming that the stress atx = Lis a constant, i.e., σT≡σxx(x=L),

σxx=

σT+Dρpνmg 2Kz

e2µKz(L−x)/D−Dρpνmg 2Kz

. (4) Previously, the threshold stressσT has been modeled as either estimated from experimental data [8], or as a constant by assuming sliding of a wedge of material [9,11]. Here, we choose to model the threshold stress σT as a φ0 dependent quantity by considering limit equilibrium of a wedge of material being displaced into the undisturbed zone, as shown inFigure 4. We assume a noncohesive Coulomb failure of the material internally, along a failure plane parallel to and meeting the surface of the transition zone. We additionally assume that the internal friction angle is also defined by µ. Limit equilibrium in the x direction can then be expressed using the notation defined in Figure 4 as Fx = Tb + Ticosθ, where Fx = DσT, Tb = µW0 = µD2ρpνmg/(2 tanθ) and Ti = µW1cosθ = µD2ρpνm20cosθ/(2 tanθ) per unit length in the ydirection.

After some rearrangement this implies that

σT= µDρpνmg

2 tanθ (1+φ02cos2θ). (5) This assumption of the failure surface introduces no new parameters into the model, and as will be shown in the following, closely predicts the measured value of σT for a large range of system parameters. In the limit whereφ0 → 0, this definition

FIGURE 4 | Limit equilibrium of the transition zone.For the pile to be displaced by a forceFx, two forces must be overcome;Tb, the basal traction due to the weightW0of the green region, and thexcomponent of the internal sliding tractionTialong the assumed failure surface denoted by the dashed line, due to the normal component of the weight above the failure surface,W1, of the blue region.

reduces to that used in Knudsen et al. [9] and Sandnes et al. [11].

Including this new definition of the threshold stress, Equation (5), in Equation (4) gives

σxx= Dρpνmg 2Kz

µKz

tanθ(1+φ02cos2θ)+1

e2µKz(L−x)/D−1

. (6) A best fit estimate is used to find Kz from Equation (6), and is shown as the dashed line inFigure 3Datx = 0, using the measured values ofνm,θ andφ0, which adequately captures the behavior of the system pastL/D = 2. Before this limit, stress redistribution has not saturated, andσxxis less than the predicted value. We find the same transition value ofL/D≈2 for all cases reported here.

The measured value of apparent frictionµ = σxzzz inside the packing, shown in Figure 3Fshows that the system is far from failure inside the plug zone, and increasingly unstable in the transition zone. The out of plane Janssen coefficient,Ky = σyyxx, shown inFigure 3G, has large variations inx, but is not significantly affected by the formation of the plug. The in plane Janssen coefficient (Figure 3H),Kzzzxx, however, is strongly influenced by the formation of the plug, and is relatively constant with increasingLinside the plug zone.

An underlying assumption of the Janssen stress redistribution is that when averaging over the width of the system (here in the y and z directions), the principal stress directions are parallel to the system geometry [4]. For this reason we measureα, the absolute value of thexcomponent of the eigenvector of the major principal stress, which is shown inFigure 3I. Whenα ≈ 1 the major principal stress points along thex-axis, and whenα ≈ 0, the principal stress lies in theyzplane. Forx≤Lwe find that the major principal stress is collinear with the system geometry, and the Janssen stress model fits well. In a traditional silo problem, gravity acts parallel to the applied stress, and averaging across the width of a silo ensures the validity of this assumption. For this case, however, because the direction of gravity has broken the inherent symmetry of the silo problem, its validity is not ensured [20]. We do, however, find that this assumption holds well for this and all simulations reported here.

3.1. Gap spacing

As motivated in Equation (6), the gap spacingDlargely controls the magnitude of the stresses within the system. For this reason, we here vary this spacing systematically fromD=1 toD=15, while maintainingφ0=0.5±0.05 andI=0.01 (except for the case ofD= 1, whereφ0 ≈ 0.66), as depicted for four values of DinFigure 5. To make a reasonable comparison between these simulations, in each case the area of the piston is kept constant, such that its area isWD=100. Select measures of the behavior of the system are shown inFigure 6. Slope angles,θ, are averaged over the times corresponding to 2D≤L≤10D, whilstKandσT are averaged temporally over values in the range 2D≤L≤10D, where at each time we measure spatially in the rangeL/4≤x≤ 3L/4. InFigures 6A,B, we observe increasing solid fraction in the plug,νm, and slope angle,θ, with increasing gap spacing, as the effect of the boundaries on the system decreases.

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FIGURE 5 | Particle positions for four simulations with varying gap spacing. Top to bottom:D=1,2,5, and 15. For all cases,φ00.5, I=0.01and the simulation is displayed at the time corresponding toL=4D.

Particles are colored by size, darker colors representing smaller particles.

For each simulation, the measured normal stress at the piston, σnp, is fitted with Equation (6), and a best fit estimate ofKzis shown as crosses, with the standard deviation of the error of the regression used as error bars, inFigure 6C. The mean and standard deviation of the measured values ofKzandKyfrom the continuum data betweenL = 2Dand L = 10Dare shown as dots and triangles, respectively. For D ≥ 2 we find that both the measured values of Kz and Ky are independent of D, and have mean values ofKy = 0.67±0.04 andKz = 0.58±0.05.

Best fit estimates of Kz are also independent of D, with mean values ofKz = 0.56±0.07.Figure 6Dshows the mean ofσT also fromL = 2 toL = 10. Triangles represent the prediction from Equation (5) using the measured values ofνm,θandφ0. In all cases, we find the measured and fitted values ofKzto be in agreement, whereas the values ofσTagree only withD≥3. We note, however, thatσTdepends strongly onθ, and we have as yet no means for predicting this quantity. The dependence ofσTonθ is in contrast to studies on fold and thrust belts [21], where there is no confinement vertically above the material.

3.2. Initial Packing Fraction

Existing models [8,9] for the evolution of the stresses in similar geometries have neglected any effect of the initial packing fraction φ0. To test this assumption, we here vary φ0 from 0.1 to 0.6, while maintaining D = 5 and I = 0.01. As shown in Figures 7A,B, the packing fraction inside the plug and the slope of the transition zone are independent of the initial packing fraction. InFigure 7C, we observe that the measured and best fit values of Kz are in agreement for a wide range of φ0, and that these values are lower than the measured values ofKy. The prediction of threshold stress from Equation (5), which includes a dependence onφ0, slightly under-predicts the threshold stress at φ0 = 0.1. Nevertheless, both the measured and predicted values of the threshold stress inFigure 7Dare in agreement with observations from Eriksen et al. [8], where a non-dimensional threshold stress of σT = 10.7 was found to reproduce the observed pattern formation behavior in the quasi-static limit, at D=5, for a range of values ofφ0≤0.5.

3.3. Inertial Number

Finally, we wish to comment on inertial effects in such a system.

Toward this end we systematically vary the inertial number I

from 10−2 to 10 while maintaining D = 5 andφ0 = 0.5± 0.05. As shown in Figure 8, a transition occurs at I ≈ 0.1, where the quasistatic behavior begins to be dominated by inertial effects, and the system is fluidized. InFigure 8A, we notice a jump in the maximum solid fraction, as the particles begin to flow and rearrange due to the increased piston velocity. This is accompanied by an increase in the slope angleθ (Figure 8B), and a decrease in the accumulation rate (Figure 8C, as the grains begin to slip relative to the walls. With increasing piston velocity, the anisotropy of the system is lost, as shown inFigure 8D, and bothKyandKztend toward a mean value of 0.56±0.02 forI≥1.

As shown inFigure 8E, the threshold stress, σT, also diverges aboveI = 0.1 away from the theoretical prediction. For values ofI ≥0.1, we have therefore used the measured value ofσTin the best fit estimation ofKzshown inFigure 8D, rather than the value predicted from Equation (5), as used in all other cases.

4. Conclusions

We have here described a large number of simulations of granular materials which have been compacted in a confined geometry.

For all cases, we observed that the stress distribution within the packing is well approximated by previous models, once a more rigorous definition of the threshold stress is used. This is true for a wide range of gap spacings, initial filling fractions and piston rates.

In this study we have used a rough boundary condition, where macroscopic friction at the piston and walls is equal to the inter-particle friction. However, in many systems we expect the roughness at the boundaries to be lower than that between particles. It is unclear how this difference will affect either the accumulation of material near the piston head, or the stress distribution within the packing.

Below a gap spacing of 3 particle diameters, the stress distribution is not well represented by this model. We conclude that D = 3 represents the smallest system size which may reasonably be described by the one dimensional Janssen stress model. In addition, at inertial numbers ofI ≥0.1, we find that there is significant slip at the boundary, and the threshold stress diverges from the model prediction. In all cases, we cannot as yet predict the slope of the free surface in the transition zone, but we observe that this slope approaches the angle of repose for large systems at low piston rates. Janssen stress coefficients for this system are well represented byKz=0.6±0.1 andKy=0.7±0.1 for a wide range of system parameters. A model for the threshold stress has been presented using limit equilibrium, and this holds well for systems withD≥3 andI<0.1.

The slope angle,θ, has been measured for different system parameters to lie in the range of 2–18.A priori, we could only assume that this angle must be smaller than or equal to the angle of repose, which for these grains is approximately 20. The wide variability ofθ is as yet unexplained, and is in contrast to the case where a top boundary does not exist, for example in fold and thrust belts [21], bulldozing [22] and additive manufacturing using loose powders [23]. We do note, however, that at large values ofDthe slope angle approaches the angle of repose.

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FIGURE 6 | Descriptors of the system with varying gap spacingD.

Error bars in each plot represent one standard deviation of the measured value.(A)Average solid fraction within the plug zone,νm.(B)Slope of the pile in the transition zone,θ.(C)Crosses represent best fit value ofKzfrom measurement of the stress on the piston head,σnpusing Equation (6).Kzand

Ky, represented by dots and triangles respectively, are calculated directly from the coarse grained granular packing.(D)Threshold stressσT. Dots represent the mean value of the coarse grained continuum fieldσxxatx=L, and crosses represent predicted values from Equation (5) using measured values ofνm,θandφ0.

FIGURE 7 | Descriptors of the system with varying initial packing fractionφ0.Error bars in each plot represent one standard deviation of the measured value.(A)Average solid fraction within the plug zone,νm.(B) Slope of the pile in the transition zone,θ.(C)Crosses represent best fit value ofKzfrom measurement of the stress on the piston head,σnpusing Equation

(6).KzandKy, represented by dots and triangles respectively, are calculated directly from the coarse grained granular packing.(D)Threshold stressσT. Dots represent the mean value of the coarse grained continuum fieldσxxat x=L, and crosses represent predicted values from Equation (5) using measured values ofνm,θandφ0.

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FIGURE 8 | Descriptors of the system with varying inertial number I. Error bars in each plot represent one standard deviation of the measured value. (A) Average solid fraction within the plug zone, νm. (B) Slope of the pile in the transition zone, θ. (C) Slope of the best fit value of L(s) denoted by black dots against prediction using incompressibilty shown as the shaded region, which denotes ± one standard deviation around the mean value for each case. (D) Crosses

represent best fit value of Kz from measurement of the stress on the piston head, σnp using Equation (6). Kz and Ky, represented by dots and triangles respectively, are calculated directly from the coarse grained granular packing. (E) Threshold stress σT. Dots represent the mean value of the coarse grained continuum field σxx atx=L, and crosses represent predicted values from Equation (5) using measured values ofνm, θ and φ0.

With regards to the two Janssen parameters, we can clearly distinguish the values of Ky and Kz in Figures 6C, 7C, 8D, for I < 0.1. The reason for the difference between these two quantities may either be due to anisotropy in the granular packing, or due to the differing boundaries in the y and z directions. As the Janssen parameters are relatively insensitive to the gap spacing D, we conclude that this anisotropy is due to the accumulation process, which creates a preferential direction within the packing. This distinction is important when considering models which account for more complex geometries, such as in Eriksen et al. [8]. For industrial applications, such as propped fractures or sand production, the stresses within a plug of grains in a horizontal crack are expected to be a function not only of the relative size of the grains to

the crack width, but also the rate of accumulation of the grains.

Author Contributions

BM conducted the simulations, post-processing and authored the paper. BS conceived the idea for the simulations. BS, GD, JE, and KM assisted with the interpretation and analysis of the simulations, and editing of the manuscript.

Acknowledgment

The authors would like to acknowledge grants 213462/F20 and 200041/S60 from the NFR.

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Conflict of Interest Statement: The authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest.

Copyright © 2015 Marks, Sandnes, Dumazer, Eriksen and Måløy. This is an open- access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) or licensor are credited and that the original publication in this journal is cited, in accordance with accepted academic practice.

No use, distribution or reproduction is permitted which does not comply with these terms.

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